Doing as FvM says is perfectly good, I just want to add that I have a software, AnTune, that is designed to aid with exactly this kind of job.
It is a software that connects with your VNA and live calculates a matching network.
It have smoothing and averaging which can be needed if measuring an active transmitter.
Semiautomatic port extension is also inbuilt, with in many cases improved result comparing to using in VNA existing port delay which in worst case only is doing phase correction.
Supports conjugate matching between two irregular impedance curves.
Automatic calculates best network topology for ideal or lossy components.
Check how I tune a passive 2.4 GHz antenna with aid of this software.
Hope this not was too much of an ad for AnTune, but it really simplifies this kind of job and it is free to try, fully functional.
Leave a 100pF capacitor on IC pin for decoupling of any DC-bias. Some chips also require external DC bias.
Try to measure on a constant carrier. It is complicated to measure impedance if the transmitter is using time-slots with delays in between.
Check that VNA can handle actual TX power level. It is expensive to blow a port of the VNA.
Avoid measuring via long PCB transmission lines as it always adds impedance errors. Forget assumed ideal 50 Ohm traces at 2.4 GHz with PCB in FR4 material. Using in VNA inbuilt port extension is then not enough.
AnTune have functions to correct for lossy transmission lines but in place calibration is always to prefer.
When doing in place calibration, do not use calibration parameters that adds an offset for "Open". Most calibrations standards adds an offset and a assumed fringing capacitance.